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Li_2S-SiS_2-LiBO_2-LiCl体系玻璃的XPS表征
作者:张瑞峰 于亚莉 高海春 房长明 张一 火焱 
单位:中国科学院长春应用化学研究所  中国科学院长春应用化学研究所  中国科学院青海盐湖研究所  中国科学院青海盐湖研究所  中国科学院青海盐湖研究所  中国科学院青海盐湖研究所 
关键词:硫氧化物玻璃  XPS表征  玻璃网络  锂离子导体 
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出版年,卷(期):页码:1992,20(3):274-279
DOI:
摘要:
本文采用光电子能谱分析方法,首次研究Li_2S-SiS_2-LiBO_2-LiCl体系硫氧化物玻璃锂离子导体的组成、结构和状态。指出在该玻璃体系中,除与硅(硼)相键合的桥硫存在外,还有不与硅(硼)相键合的非桥硫存在;玻璃中的硫取代了氧的位置,进入玻璃网络中使结构紧密交联。对网络中的元素状态,成键及性能进行了讨论。
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The composition, structure and state of oxysulfide glassy lithium ion conductors for Li_2S-SiS_2-LiBO_2-LiCl system were studied by means of XPS.The result of XPS shows that in the glass, the partial sulfur atoms replaced oxygen place in glassy bond with boron atoms and exist in the form of bridging sulfur to produce a more highly cross-linked and stable glass network. The elements state in the glass network and bonding mechanism were discussed.
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参考文献:
[1] Button D P. J. Non-cryst. Solids, 1980, 42:297 [2] Jazarel A E. Ann. Chem. Ft., 1982, 285 [3] 陈德康,张家权.特种玻璃,1987,4:8 [4] Wada H, Menetrier Met al. Mater. Res. Bull., 1983, 18:189 [5] Angen C A. Mater. Sci. Forym., 1985, 5:139 [6] Barmer S, Guittard M. J. Mater. Res. Bull., 1984, 19:837 [7] 房长明,高海春,火焱等.硅酸盐学报,1992,20(1) :68 [8] Machiba N et al. J. Am. Ceram. Soc.,1988, 79:784 [9] Magner C Oet al. Handbook of X-ray Photoelectron Spectroscopy, Minesota: Perkin-Elmer cor-poration, 1979:56
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