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钢纤维-水泥基界面过渡区纳米力学性能
作者:徐礼华 余红芸 池寅 邓方茜 胡杰 
单位:武汉大学土木建筑工程学院 武汉 430072 
关键词:纳米力学性能 扫描电子显微镜 界面过渡区 微观结构 
分类号:TU525.9
出版年,卷(期):页码:2016,44(8):0-0
DOI:10.14062/j.issn.0454-5648.2016.08.09
摘要:

研究不同水灰比条件下的钢纤维增强水泥基复合材料界面过渡区(ITZ)的纳米力学性能。通过纳米压痕试验,测试界面过渡区及其附近区域的荷载–压痕深度曲线,运用Oliver-Pharr方法研究了弹性模量和硬度分布规律并绘制相应的微结构表征云图,结合扫描电子显微镜分析ITZ形成机制。此外,利用反褶积法对ITZ的弹性模量及压痕硬度的频率分布曲线进行多峰拟合,得到了各相的频率分布。结果表明:不同水灰比样品界面过渡区的厚度均为40 μm左右;在界面过渡区内,弹性模量和压痕硬度的最弱点在距纤维表面20 μm附近,且水灰比越大,弹性模量与压痕硬度值越小;随着水灰比的增大,界面过渡区孔洞和低密度水化硅酸钙含量逐渐增高,高密度水化硅酸钙含量逐渐降低。
 

The nanoscale mechanical properties of interfacial transition zone (ITZ) in steel fiber reinforced cementitious composite for different water/cement ratios were investigated. The P-h curves of ITZ were determined via nanoindentation test. The distribution of elastic modulus and hardness were calculated and mapped in a 2D plane by the Oliver-Pharr method. The formation mechanism of ITZ was analyzed. In addition, the frequency distribution of different phases in ITZ was determined by a multi-peak fitting deconvolution method. The result indicate that there is a interface width about 40 μm in all the cases. The minimum modulus and hardness occur at a distance of 20μm from the steel fiber surface. The greater the water/cement ratio, the lower elastic modulus and hardness will be. The content of porosity and low density C-S-H gradually increase, and the density of C-S-H decreases with the increase of water/cement ratio.
 

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基金项目:
国家自然科学基金(51478367)资助。
作者简介:
徐礼华(1962―),女,博士,教授。
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